Citation:
Zheng Jie HE, Ju Xiang LIU, Zheng Hong ZHOU, Chu Chi TANG. The Isomerization/Chlorination of O,O-D iallyl Thiophosphoric (-nic) Acid Esters with Phosphorus Oxychloride——A New Convenient Method for Synthesis of S-Alkyl Thiophosphoric(-nic) Acid Derivatives[J]. Chinese Chemical Letters,
;1998, 9(10): 903-905.
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The isomerization/chlorination of 0,0-diallyl thiophosphoric(-nic) acid esters with phosphrus oxychloride gives S-allyl thiophosphoro(-no)chloride, which reacts with substituted phenol in chloroform in the presence of triethylamine to afford eighteen new S-allyl thiophosphoric(-nic) acid derivatives. Thus, a new convenient method has been provided for synthesis of the title compounds.
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