Citation: Qingxuan Kong, Changwei Jiang, Bin Lyu, Zhaoting Li, Ning Jiao, Song Song. Denitrative iodination of nitroarenes with hydroiodic acid[J]. Chinese Chemical Letters, ;2025, 36(10): 111444. doi: 10.1016/j.cclet.2025.111444 shu

Denitrative iodination of nitroarenes with hydroiodic acid

Qingxuan Kong ^a ,
Changwei Jiang ^a ,
Bin Lyu ^a ,
Zhaoting Li ^a ,
Ning Jiao ^a ,
Song Song ^{a, b, *,}

a.
State Key Laboratory of Natural and Biomimetic Drugs, School of Pharmaceutical Sciences, Peking University, Beijing 100191, China
b.
Department of Pharmacy, Peking University First Hospital, Beijing 100034, China

ssong@bjmu.edu.cn

Received Date: 8 April 2025
Revised Date: 30 May 2025
Accepted Date: 10 June 2025
Available Online: 11 June 2025

Figures(4)

We herein present an efficient denitrative iodination method of (hetero)nitroarenes mediated by commercially available and cost-effective hydroiodic acid (HI). During the reaction process, HI plays its dual roles as both the sustainable reductant of nitro group and iodine source in the iodination step, which successfully integrates three steps into a one-pot procedure and significantly simplifies the reaction system. This approach enables a smooth metal-free conversion of nitroarenes to corresponding aryl iodides via one-pot process, exhibits a broad substrate scope and good reaction efficiency, and was conveniently applied in the concise synthesis of pharmaceuticals.
- Denitrative reaction,
- Sandmeyer reaction,
- Iodination,
- Nitroarenes,
- Aryl iodides
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沈阳化工大学材料科学与工程学院沈阳 110142