Citation: Rui Su, Xiaowei Fang, Peng Zeng, Yong Qian, Xuanzhu Li, Huiyu Xing, Jiamei Lin, Jiaquan Xu. Mass spectrometry for non-destructive detection of the average diameter of micro copper wires[J]. Chinese Chemical Letters, ;2025, 36(10): 110748. doi: 10.1016/j.cclet.2024.110748 shu

Mass spectrometry for non-destructive detection of the average diameter of micro copper wires

Rui Su ^{a, c} ,
Xiaowei Fang ^a ,
Peng Zeng ^a ,
Yong Qian ^b ,
Xuanzhu Li ^d ,
Huiyu Xing ^a ,
Jiamei Lin ^b ,
Jiaquan Xu ^{b, *,}

a.
Academician Workstation, Jiangxi University of Chinese Medicine, Nanchang 330004, China
b.
Jiangxi Key Laboratory for Mass Spectrometry and Instrumentation, East China University of Technology, Nanchang 330013, China
c.
State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, College of Chemistry, Jilin University, Changchun 130012, China
d.
Jilin Ginseng Academy, Changchun University of Chinese Medicine, Changchun 130017, China

jiaquan_xu@foxmail.com

Received Date: 13 June 2024
Revised Date: 25 October 2024
Accepted Date: 11 December 2024
Available Online: 12 December 2024

Figures(3)

The performance and price of copper-based micro linear products are determined by the diameter uniformity. How to accurately detect the wire diameter of long-length copper based micro linear products without cutting or damage has always been a technical concern for production enterprises. Herein, a novel approach was developed for nondestructive detection of the average diameter at any given segment of a long copper wire by assessing the adsorption capacity of arginine on its surface. The amount of adsorbent on the surface of the copper wire exhibits a positive correlation with the area, which can be detected by extractive electrospray ionization mass spectrometry (EESI-MS) after online elution with ammonia. The experimental results demonstrated that the analysis can be completed within 15 min, with a good linear relationship between copper wires with different diameters and the adsorption capacity of arginine. The linear correlation coefficient R² was 0.995, the relative standard deviation was 1.10%-2.81%, and the detection limit reached 2.5 µm (length of segment = 4 cm), showing potential applications for facile measurement of the average diameter of various metal wires.
- Measurement of diameter,
- Mass spectrometry,
- Non-destructive detection,
- Copper wire,
- Average diameter
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