Citation: Da-Zhong Shen, Ting-Ting Cai, Xi-Lei Zhu, Xiao-Long Ma, Ling-Qiang Kong, Qi Kang. Monitoring iodine adsorption onto zeolitic-imidazolate framework-8 film using a separated-electrode piezoelectric sensor[J]. Chinese Chemical Letters, ;2015, 26(8): 1022-1025. doi: 10.1016/j.cclet.2015.04.029 shu

Monitoring iodine adsorption onto zeolitic-imidazolate framework-8 film using a separated-electrode piezoelectric sensor

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The Key Lab in Molecular and Nano-materials Probes of the Ministry of Education of China, College of Chemistry, Chemical Engineering and Materials Science, Shandong Normal University, Jinan 250014, China

Corresponding author: Qi Kang,
Received Date: 5 January 2015
Available Online: 3 April 2015
Fund Project: The authors gratefully acknowledge financial support by National Natural Science Foundation of China (Nos. 21175084, 21275091) (Nos. 21175084, 21275091) Ministry of Education (No. KLCBTCMR2001-01) (Hunan Normal University)Research Fund for the Doctoral Program of Higher Education of China (No. 20113704110003). (No. KLCBTCMR2001-01)

In this work, a separated-electrode piezoelectric sensor (SEPS), constructed by a naked quartz crystal mounted between two electrodes, is reported for applications in a corrosive gaseous phase. The response of SEPS was measured by an impedance analysis method. It was shown that SEPS has an excellent frequency stability because its quality factor is in the order of 10⁵. The SEPS can be operated even with the electrode gap in air larger than 1 cm. Compared with a conventional quartz crystal microbalance, the resonant frequency of the SEPS is independent of the mass change in the electrode. The SEPS was applied to monitor the adsorption of iodine on quartz surface and zeolitic-imidazolate framework-8 (ZIF-8) film as well as in the transfer of iodine between two ZIF-8 films. The SEPS offers the advantages of easy preparation, corrosion-resistant and convenience in combination with mass and optical measurements.
- Separated-electrode,
- Piezoelectric sensor,
- Iodine adsorption,
- Zeolitic-imidazolate framework
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沈阳化工大学材料科学与工程学院沈阳 110142