Determination of petroleum sulfonates in crude oil by column-switching anion-exchange chromatography

Liang Zhao Xu Long Cao Hong Yan Wang Xia Liu Sheng Xiang Jiang

引用本文: Liang Zhao,  Xu Long Cao,  Hong Yan Wang,  Xia Liu,  Sheng Xiang Jiang. Determination of petroleum sulfonates in crude oil by column-switching anion-exchange chromatography[J]. Chinese Chemical Letters, 2008, 19(2): 219-222. doi: 10.1016/j.cclet.2007.12.015 shu
Citation:  Liang Zhao,  Xu Long Cao,  Hong Yan Wang,  Xia Liu,  Sheng Xiang Jiang. Determination of petroleum sulfonates in crude oil by column-switching anion-exchange chromatography[J]. Chinese Chemical Letters, 2008, 19(2): 219-222. doi: 10.1016/j.cclet.2007.12.015 shu

Determination of petroleum sulfonates in crude oil by column-switching anion-exchange chromatography

  • 基金项目:

    We are grateful to the National Nature Science Foundation of China (No. 20675085). We are also grateful to the support from the Program of the Light in China's Western Region (2003) and the Province Nature Science Foundation of Gansu (No. 3ZS041-A25-23).

摘要: A column-switching anion-exchange chromatography method was described for the separation and determination of petroleum monosulfonates (PMS) and petroleum disulfonates (PDS) in crude oil that was simply diluted with the dichloromethane/methanol (60/40).The high performance liquid chromatography (HPLC) system consisted of a clean-up column and an analytical column, which were connected with two six-port switching valves.Detection of petroleum sulfonates was available and repeatable.This method has been successfully applied to determine PMS and PDS in crude oil samples from Shengli oil field.

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  • 收稿日期:  2007-10-11
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