English

• 
  
• 1. [1]

     Cui, K.; Ma, Z.; Tian, N.; Su, F.; Liu, D.; Li, L. Multiscale and multistep ordering of flow-induced nucleation of polymers. Chem. Rev. 2018, 118(4), 1840−1886 doi: 10.1021/acs.chemrev.7b00500

  2. [2]

     Tang, Y. J.; Jiang, Z. Y.; Enderle, H. F.; Lilge, D.; Roth, S. V.; Gehrke, R.; Rieger, J.; An, L. J.; Men, Y. F. Mapping the damaged zone around the crack tip in high density polyethylene with synchrotron microfocus small angle X-ray scattering technique. Chinese J. Polym. Sci. 2010, 28(2), 165−170 doi: 10.1007/s10118-010-8243-6

  3. [3]

     Lu, Y.; Sun, Y. Y.; Chen, R.; Li, X. H.; Men, Y. F. Deformation temperature and lamellar thickness dependency of Form I to Form III phase transition in syndiotactic polypropylene during tensile stretching. Chinese J. Polym. Sci. 2014, 32(9), 1210−1217 doi: 10.1007/s10118-014-1494-x

  4. [4]

     Xu, J. Z.; Chen, C.; Wang, Y.; Tang, H.; Li, Z. M.; Hsiao, B. S. Graphene nanosheets and shear flow induced crystallization in isotactic polypropylene nanocomposites. Macromolecules 2011, 44(8), 2808−2818 doi: 10.1021/ma1028104

  5. [5]

     Portale, G.; Hermida-Merino, D.; Bras, W. Polymer research and synchrotron radiation perspectives. Eur. Polym. J. 2016, 81, 415−432 doi: 10.1016/j.eurpolymj.2016.04.015

  6. [6]

     Thurman, D. W.; Fernandez-Ballester, L.; Oberhauser, J. P.; Kornfield, J. A. Shear-mediated crystallization of isotactic polypropylene: A wide angle X-ray study of the role of long chains. Abstracts of Papers of the American Chemical Society 2004, 228, U442

  7. [7]

     Kumaraswamy, G.; Verma, R. K.; Kornfield, J. A.; Yeh, F.; Hsiao, B. S. Shear-enhanced crystallization in isotactic polypropylene. In situ synchrotron SAXS and WAXD. Macromolecules 2004, 37(24), 9005−9017 doi: 10.1021/ma035840n

  8. [8]

     Wang, Z.; Hsiao, B. S.; Sirota, E. B.; Agarwal, P.; Srinivas, S. Probing the early stages of melt crystallization in polypropylene by simultaneous small- and wide- angle X-ray scattering and laser light scattering. Macromolecules 2000, 33(3), 978−989 doi: 10.1021/ma991468t

  9. [9]

     Ma, Z.; Balzano, L.; Peters, G. W. Dissolution and re-emergence of flow-induced shish in polyethylene with a broad molecular weight distribution. Macromolecules 2016, 49(7), 2724−2730 doi: 10.1021/acs.macromol.6b00333

  10. [10]

      Ma, Z.; Fernandez-Ballester, L.; Cavallo, D.; Gough, T.; Peters, G. W. M. High-stress shear-induced crystallization in isotactic polypropylene and propylene/ethylene random copolymers. Macromolecules 2013, 46(7), 2671−2680 doi: 10.1021/ma302518c

  11. [11]

      Cui, K.; Meng, L.; Ji, Y.; Li, J.; Zhu, S.; Li, X.; Tian, N.; Liu, D.; Li, L. Extension-induced crystallization of poly(ethylene oxide) bidisperse blends: an entanglement network perspective. Macromolecules 2014, 47(2), 677−686 doi: 10.1021/ma402031m

  12. [12]

      Liu, D.; Tian, N.; Cui, K.; Zhou, W.; Li, X.; Li, L. Correlation between flow-induced nucleation morphologies and strain in polyethylene: from uncorrelated oriented point-nuclei, scaffold-network, and microshish to shish. Macromolecules 2013, 46(9), 3435−3443 doi: 10.1021/ma400024m

  13. [13]

      Liu, Y.; Cui, K.; Tian, N.; Zhou, W.; Meng, L.; Li, L.; Ma, Z.; Wang, X. Stretch-induced crystal-crystal transition of polybutene-1: an in situ synchrotron radiation wide-angle X-ray scattering study. Macromolecules 2012, 45(6), 2764−2772 doi: 10.1021/ma2026513

  14. [14]

      Cui, K. P.; Meng, L. P.; Tian, N.; Zhou, W. Q.; Liu, Y. P.; Wang, Z.; He, J.; Li, L. B. Self-acceleration of nucleation and formation of shish in extension-induced crystallization with strain beyond fracture. Macromolecules 2012, 45(13), 5477−5486 doi: 10.1021/ma300338c

  15. [15]

      Matsuba, G.; Zhao, Y. F.; Teratani, M.; Hayashi, Y.; Takayama, Y.; Ogino, Y.; Nishida, K.; Kanaya, T. Oriented structure in isotactic polystyrene melt induced by shear flow. Kobunshi Ronbunshu 2009, 66(10), 419−427 doi: 10.1295/koron.66.419

  16. [16]

      Yan, S.; Wu, Z.; Yu, H.; Gong, Y.; Tan, Y.; Du, R.; Chen, W.; Xing, X.; Mo, G.; Chen, Z. Time-resolved small-angle X-ray scattering study on the growth behavior of silver nanoparticles. J. Phys. Chem. C 2014, 118(21), 11454−11463 doi: 10.1021/jp502482c

  17. [17]

      Meng, L. P.; Chen, X. W.; Lin, Y. F.; Li, L. B. Improving the softness of BOPP films: from laboratory investigation to industrial processing. Chinese J. Polym. Sci. 2017, 35(9), 1122−1131 doi: 10.1007/s10118-017-1965-y

  18. [18]

      Wang, Z.; Ma, Z.; Li, L. Flow-induced crystallization of polymers: molecular and thermodynamic considerations. Macromolecules 2016, 49(5), 1505−1517 doi: 10.1021/acs.macromol.5b02688

  19. [19]

      Ma, Z.; Balzano, L.; Erp, T. V.; Portale, G.; Peters, G. W. M. Short-term flow induced crystallization in isotactic polypropylene: how short is short? Macromolecules 2013, 46(23), 9249−9258 doi: 10.1021/ma401833k

  20. [20]

      Li, Z.; Wu, Z.; Mo, G.; Xing, X.; Liu, P. A small-angle X-ray scattering station at Beijing synchrotron radiation facility. Instrum. Sci. Technol. 2014, 42(2), 128−141 doi: 10.1080/10739149.2013.845845

  21. [21]

      Wang, Z.; Ju, J.; Meng, L.; Tian, N.; Chang, J.; Yang, H.; Ji, Y.; Su, F.; Li, L. Structural and morphological transitions in extension-induced crystallization of poly(1-butene) melt. Soft Matter 2017, 13(19), 3639−3648 doi: 10.1039/C7SM00107J

  22. [22]

      Cui, K.; Liu, D.; Ji, Y.; Huang, N.; Ma, Z.; Wang, Z.; Lv, F.; Yang, H.; Li, L. Nonequilibrium nature of flow-induced nucleation in isotactic polypropylene. Macromolecules 2015, 48(3), 694−699 doi: 10.1021/ma502412y

  23. [23]

      Liu, Y.; Zhou, W.; Cui, K.; Tian, N.; Wang, X.; Liu, L.; Li, L.; Zhou, Y. Extensional rheometer for in-situ X-ray scattering study on flow-induced crystallization of polymer. Rev. Sci. Instrum. 2011, 82(4), 045104 doi: 10.1063/1.3574219

  24. [24]

      Meng, L.; Li, J.; Cui, K.; Chen, X.; Lin, Y.; Xu, J.; Li, L. A simple constrained uniaxial tensile apparatus for in-situ investigation of film stretching processing. Rev. Sci. Instrum. 2013, 84(11), 115104 doi: 10.1063/1.4828665

  25. [25]

      Zhang, R.; Ji, Y. X.; Zhang, Q. L.; Ju, J. Z.; Sarmad, A.; Li, L. F.; Zhao, H. Y.; Li, L. B. A universal blown film apparatus for in situ X-ray measurements. Chinese J. Polym. Sci. 2017, 35(12), 1508−1516 doi: 10.1007/s10118-017-2000-z

  26. [26]

      Yan, T.; Zhao, B.; Cong, Y.; Fang, Y.; Cheng, S.; Li, L.; Pan, G.; Wang, Z.; Li, X.; Bian, F. Critical strain for shish-kebab formation. Macromolecules 2009, 43(2), 602−605

  27. [27]

      Wang, Z. The non-equilibrium phase diagrams of flow-induced crystallization and melting of polyethylene. Sci. Rep. 2016, 6, 32968 doi: 10.1038/srep32968

  28. [28]

      Ju, J.; Wang, Z.; Su, F.; Ji, Y.; Yang, H.; Chang, J.; Ali, S.; Li, X.; Li, L. Extensional flow-induced dynamic phase transitions in isotactic polypropylene. Macromol. Rapid Commun. 2016, 37(17), 1441−1445 doi: 10.1002/marc.v37.17

  29. [29]

      Chen, X.; Lv, F.; Su, F.; Ji, Y.; Meng, L.; Wan, C.; Lin, Y.; Li, X.; Li, L. Deformation mechanism of iPP under uniaxial stretching over a wide temperature range: An in-situ synchrotron radiation SAXS/WAXS study. Polymer 2017, 118, 12−21 doi: 10.1016/j.polymer.2017.04.054

  30. [30]

      Chen, L.; Zhou, W.; Su, F.; Zhang, W.; Chen, P.; Ji, Y.; Li, L. Filler-induced heterogeneous distribution of stretch-induced crystallization in natural rubber: An in-situ synchrotron-radiation micro-focused scanning X-ray diffraction study. Polymer 2017, 115, 217−223 doi: 10.1016/j.polymer.2017.03.043

  31. [31]

      Lin, Y.; Meng, L.; Wu, L.; Li, X.; Chen, X.; Zhang, Q.; Zhang, R.; Zhang, W.; Li, L. A semi-quantitative deformation model for pore formation in isotactic polypropylene microporous membrane. Polymer 2015, 80, 214−227 doi: 10.1016/j.polymer.2015.10.067

  32. [32]

      Lin, Y.; Li, X.; Meng, L.; Chen, X.; Lv, F.; Zhang, Q.; Zhang, R.; Li, L. Structural evolution of hard-elastic isotactic polypropylene film during uniaxial tensile deformation: the effect of temperature. Macromolecules 2018, 51(7), 2690−2705 doi: 10.1021/acs.macromol.8b00255

  33. [33]

      Lv, F.; Chen, X.; Wan, C.; Su, F.; Ji, Y.; Lin, Y.; Li, X.; Li, L. Deformation of ultrahigh molecular weight polyethylene precursor fiber: crystal slip with or without melting. Macromolecules 2017, 50(17), 6385−6395 doi: 10.1021/acs.macromol.7b01153

  34. [34]

      Li, X.; Lin, Y.; Su, F.; Chen, X.; Lv, F.; Meng, L.; Zhang, Q.; Li, L. Stabilization mechanism of micropore in high-density polyethylene: a comparison between thermal and mechanical pathways. Macromol. Mater. Eng. 2017, 302(10), 1700178 doi: 10.1002/mame.v302.10

  35. [35]

      Li, X.; Meng, L.; Lin, Y.; Chen, X.; Zhang, Q.; Zhang, R.; Wu, L.; Zhang, W.; Li, L. Preparation of highly oriented polyethylene precursor film with fibril and its influence on microporous membrane formation. Macromol. Chem. Phys. 2016, 217(8), 974−986 doi: 10.1002/macp.v217.8

  36. [36]

      Li, X.; Lin, Y.; Ji, Y.; Meng, L.; Zhang, Q.; Zhang, R.; Zhang, W.; Li, L. Strain and temperature dependence of deformation mechanism of lamellar stacks in HDPE and its guidance on microporous membrane preparation. Polymer 2016, 105, 264−275 doi: 10.1016/j.polymer.2016.10.043

  37. [37]

      Lin, Y.; Li, X.; Meng, L.; Chen, X.; Lv, F.; Zhang, Q.; Zhang, R.; Li, L. Structural evolution of hard-elastic isotactic polypropylene film during uniaxial tensile deformation: the effect of temperature. Macromolecules 2018, 51(7), 2690−2705 doi: 10.1021/acs.macromol.8b00255

  38. [38]

      Kanaya, T.; Polec, I. A.; Fujiwara, T.; Inoue, R.; Nishida, K.; Matsuura, T.; Ogawa, H.; Ohta, N. Precursor of shish-kebab above the melting temperature by microbeam X-ray scattering. Macromolecules 2013, 46(8), 3031−3036 doi: 10.1021/ma400061a

  39. [39]

      Gutiérrez, M. C. G.; Alfonso, G. C.; Riekel, C.; Azzurri, F. Spatially resolved flow-induced crystallization precursors in isotactic polystyrene by simultaneous small- and wide-angle X-ray microdiffraction. Macromolecules 2004, 37(2), 478−485 doi: 10.1021/ma0350157

  40. [40]

      Su, F. M.; Li, X. Y.; Zhou, W. M.; Zhu, S. S.; Ji, Y. X.; Wang, Z.; Qi, Z. M.; Li, L. B. Direct formation of isotactic poly(1-butene) form I crystal from memorized ordered melt. Macromolecules 2013, 46(18), 7399−7405 doi: 10.1021/ma400952r

  41. [41]

      Zhou, W.; Li, X.; Lu, J.; Huang, N.; Chen, L.; Qi, Z.; Li, L.; Liang, H. Toughening mystery of natural rubber deciphered by double network incorporating hierarchical structures. Sci. Rep. 2014, 4, 7502

  42. [42]

      Melnikov, A.; Rosenthal, M.; Rodygin, A.; Doblas, D.; Anokhin, D.; Burghammer, M.; Ivanov, D. Re-exploring the double-melting behavior of semirigid-chain polymers with an in-situ combination of synchrotron nano-focus X-ray scattering and nanocalorimetry. Eur. Polym. J. 2016, 81, 598−606 doi: 10.1016/j.eurpolymj.2015.12.031

  43. [43]

      Su, F.; Zhou, W.; Li, X.; Ji, Y.; Cui, K.; Qi, Z.; Li, L. Flow-induced precursors of isotactic polypropylene: an in situ time and space resolved study with synchrotron radiation scanning X-ray microdiffraction. Macromolecules 2014, 47(13), 4408−4416 doi: 10.1021/ma5005293

  44. [44]

      Su, F.; Ji, Y.; Meng, L.; Chang, J.; Chen, L.; Li, L. Shear-induced precursors in polyethylene: An in-situ synchrotron radiation scanning X-ray microdiffraction study. Polymer 2018, 135, 61−68 doi: 10.1016/j.polymer.2017.12.021

  45. [45]

      Chen, L.; Chen, W.; Zhou, W.; Li, J.; Liu, Y.; Qi, Z.; Li, L. In situ microscopic infrared imaging study on deformation-induced spatial orientation and phase transition distributions of PA12. J. Appl. Polym. Sci. 2014, 131(17), 40703

  46. [46]

      Chen, L.; Song, L.; Li, J.; Chen, P.; Huang, N.; Li, L. From the volume-filling effect to the stress-bearing network: the reinforcement mechanisms of carbon black filler in natural rubber. Macromol. Mater. Eng. 2016, 301(11), 1390−1401 doi: 10.1002/mame.v301.11

  47. [47]

      Chen, L.; Zhou, W.; Lu, J.; Li, J.; Zhang, W.; Huang, N.; Wu, L.; Li, L. Unveiling reinforcement and toughening mechanism of filler network in natural rubber with synchrotron radiation X-ray nano-computed tomography. Macromolecules 2015, 48(21), 7923−7928 doi: 10.1021/acs.macromol.5b01301

  48. [48]

      Song, L.; Wang, Z.; Tang, X.; Chen, L.; Chen, P.; Yuan, Q.; Li, L. Visualizing the toughening mechanism of nanofiller with 3D X-ray nano-CT: stress-induced phase separation of silica nanofiller and silicone polymer double networks. Macromolecules 2017, 50(18), 7249−7257 doi: 10.1021/acs.macromol.7b00539

  49. [49]

      Ellis, G. J.; Martin, M. C. Opportunities and challenges for polymer science using synchrotron-based infrared spectroscopy. Eur. Polym. J. 2016, 81, 505−531 doi: 10.1016/j.eurpolymj.2016.02.013

  50. [50]

      Geng, Y.; Wang, G.; Cong, Y.; Bai, L.; Li, L.; Yang, C. Shear-induced nucleation and growth of long helices in supercooled isotactic polypropylene. Macromolecules 2009, 42(13), 4751−4757 doi: 10.1021/ma9004567

  51. [51]

      An, H.; Li, X.; Geng, Y.; Wang, Y.; Wang, X.; Li, L.; Li, Z.; Yang, C. Shear-induced conformational ordering, relaxation, and crystallization of isotactic polypropylene. J. Phys. Chem. B 2008, 112(39), 12256−12262 doi: 10.1021/jp802511b

  52. [52]

      An, H.; Zhao, B.; Ma, Z.; Shao, C.; Wang, X.; Fang, Y.; Li, L.; Li, Z. Shear-induced conformational ordering in the melt of isotactic polypropylene. Macromolecules 2007, 40(14), 4740−4743 doi: 10.1021/ma071021h

  53. [53]

      Santoro, G.; Ochando, I. M.; Ellis, G. Advanced vibrational microspectroscopic study of conformational changes within a craze in poly(ethylene terephthalate). Macromolecules 2015, 48(4), 1162−1168 doi: 10.1021/ma502193t

  54. [54]

      Dumas, P.; Jamin, N.; Teillaud, J.; Miller, L.; Beccard, B. Imaging capabilities of synchrotron infrared microspectroscopy. Faraday Discuss. 2004, 126, 289−302 doi: 10.1039/b305065c

  55. [55]

      Li, H.; Zhou, W.; Ji, Y.; Hong, Z.; Miao, B.; Li, X.; Zhang, J.; Qi, Z.; Wang, X.; Li, L.; Li, Z. M. Spatial distribution of crystal orientation in neck propagation: An in-situ microscopic infrared imaging study on polyethylene. Polymer 2013, 54(2), 972−979 doi: 10.1016/j.polymer.2012.12.012

  56. [56]

      Su, F. M.; Li, X. Y.; Zhou, W. M.; Chen, W.; Li, H. L.; Cong, Y. H.; Hong, Z. H.; Qi, Z. M.; Li, L. B. Accelerating crystal-crystal transition in poly(1-butene) with two-step crystallization: An in-situ microscopic infrared imaging and microbeam X-ray diffraction study. Polymer 2013, 54(13), 3408−3416 doi: 10.1016/j.polymer.2013.04.046

  57. [57]

      Hong, Z.; Cong, Y.; Qi, Z.; Li, H.; Zhou, W.; Chen, W.; Wang, X.; Zhou, Y.; Li, L. Studying deformation behavior of a single spherulite with in-situ infrared microspectroscopic imaging. Polymer 2012, 53(2), 640−647 doi: 10.1016/j.polymer.2011.12.009

  58. [58]

      Li, J.; Li, H.; Meng, L.; Li, X.; Chen, L.; Chen, W.; Zhou, W.; Qi, Z.; Li, L. In-situ MR imaging on the plastic deformation of iPP thin films. Polymer 2014, 55(5), 1103−1107 doi: 10.1016/j.polymer.2014.01.033

  59. [59]

      Cong, Y.; Hong, Z.; Zhou, W.; Chen, W.; Su, F.; Li, H.; Li, X.; Yang, K.; Yu, X.; Qi, Z. Conformational ordering on the growth front of isotactic polypropylene spherulite. Macromolecules 2012, 45(21), 8674−8680 doi: 10.1021/ma301595k

  60. [60]

      Ling, S.; Qi, Z.; Knight, D. P.; Shao, Z.; Chen, X. Synchrotron FTIR microspectroscopy of single natural silk fibers. Biomacromolecules 2011, 12(9), 3344−3349 doi: 10.1021/bm2006032

  61. [61]

      Cong, Y. H.; Hong, Z. H.; Qi, Z. M.; Zhou, W. M.; Li, H. L.; Liu, H.; Chen, W.; Wang, X.; Li, L. B. Conformational ordering in growing spherulites of isotactic polypropylene. Macromolecules 2010, 43(23), 9859−9864 doi: 10.1021/ma1019686

  62. [62]

      Chen, X.; Shao, Z.; Marinkovic, N. S.; Miller, L. M.; Zhou, P.; Chance, M. R. Conformation transition kinetics of regenerated Bombyx mori silk fibroin membrane monitored by time-resolved FTIR spectroscopy. Biophys. Chem. 2001, 89(1), 25−34 doi: 10.1016/S0301-4622(00)00213-1

  63. [63]

      Lewis, E. N.; Treado, P. J.; Reeder, R. C.; Story, G. M.; Dowrey, A. E.; Marcott, C.; Levin, I. W. Fourier transform spectroscopic imaging using an infrared focal-plane array detector. Anal. Chem. 1995, 67(19), 3377−3381 doi: 10.1021/ac00115a003

  64. [64]

      Liu, F.; Brady, M. A.; Wang, C. Resonant soft X-ray scattering for polymer materials. Eur. Polym. J. 2016, 81, 555−568 doi: 10.1016/j.eurpolymj.2016.04.014

  65. [65]

      Qi, F. Combustion chemistry probed by synchrotron VUV photoionization mass spectrometry. P. Combust. Inst. 2013, 34(1), 33−63 doi: 10.1016/j.proci.2012.09.002

  66. [66]

      Sikharulidze, I.; Dolbnya, I. P.; Fera, A.; Madsen, A.; Ostrovskii, B. I.; de Jeu, W. H. Smectic membranes in motion: Approaching the fast limits of X-ray photon correlation spectroscopy. Phys. Rev. Lett. 2002, 88(11), 115503 doi: 10.1103/PhysRevLett.88.115503

•