Citation: Min Min LIANG, Mei Ling QI, Ruo Nong FU. Flash Evaporation and Headspace Solid-phase Microextraction for the Analysis of the Essential Oils in Traditional Chinese Medicine, Houttuynia Cordata Thunb[J]. Chinese Chemical Letters, ;2005, 16(5): 659-662. shu

Flash Evaporation and Headspace Solid-phase Microextraction for the Analysis of the Essential Oils in Traditional Chinese Medicine, Houttuynia Cordata Thunb

Department of Chemistry, School of Science, Beijing Institute of Technology, Beijing 100081

Received Date: 24 May 2004

Fund Project: This research work was financially supported by the Key Project of National Science and Technology Ministry of China (No.2002DEA20021-3, 2002BA906A29).

We have investigated the use of flash evaporation, headspace solid-phase microextraction (HS-SPME) and steam distillation (SD) as sample concentration and preparation techniques for the analysis of volatile constituents present in Houttuynia cordata Thunb. The samples were analyzed by gas chromatography (GC) and identified by mass spectrometry (MS).Comparison studies were performed. It was found that the results obtained between Headspace solid-phase microextraction HS-SPME and SD techniques were in good agreement. Seventy-nine compounds in Houttuynia cordata Thunb were identified by MS. In flash evaporation, thirty-nine compounds were identified. Discrimination in the response for many constituents studied was not observed, which can be clearly observed in SD and HS-SPME techniques. As a conclusion,HS-SPME is a powerful tool for determining the volatile constitutes present in the Houttuynia cordata.
- Headspace solid-phase microextraction,
- flash evaporation,
- essential oils,
- GC-MS
1. [1]
  Bohao Liu , Xue Jiang , Ruizhi Ning , Heng Zhao , Yanpeng Zhang , Junnan Zhang , Tianqing Liu , Danyao Qu , Yinhui Bao , Zhanchen Guo , Xiaoyan Zeng , Shan Gao , Kun Fan , Runyi Tao , Jian Ji , Guangjian Zhang , Weiwei Wu . Tedlar bag free: Accurate volatolomics of ⅠA stage non-small cell lung cancer come out in wash. Chinese Chemical Letters, 2025, 36(6): 110301-. doi: 10.1016/j.cclet.2024.110301
2. [2]
  Jiawen Zhu , Yingge Hao , Zhen Song , Huina Zhou , Youmei Wang , Ling Yan , Minghua Lu . Synthesis of mesopore-rich hollow carbon nanospheres as headspace solid-phase microextraction coating to extract PAHs from water and honey. Chinese Chemical Letters, 2025, 36(12): 111290-. doi: 10.1016/j.cclet.2025.111290
3. [3]
  Junfeng Huang , Hongxin Chen , Yan Liao , Xiaowen Zhang , Zengzhu Zhang , Xiaoyu Su , Zihong Xie , Biao Li , Baode Shen , Pengfei Yue . Metal-organic framework materials for encapsulation, release and delivery of essential oils: Engineering strategies and challenges. Chinese Chemical Letters, 2026, 37(3): 112049-. doi: 10.1016/j.cclet.2025.112049
4. [4]
  Jisung Yoon , Junghum Park , Hojae Lee , Sang won Lee , Miju Ku , Junseop Lee , Jonghyuck Lee , Tae ho Shin , Young-Beom Kim . Enhancing the electrochemical performance of Ni-based electrodes via flash light sintering for metal-supported solid oxide fuel cells (MS-SOFCs). Chinese Journal of Structural Chemistry, 2025, 44(12): 100758-100758. doi: 10.1016/j.cjsc.2025.100758
5. [5]
  Hao Sun , Xiaoxue Li , Baoyu Wu , Kai Zhu , Yinyi Gao , Tianzeng Bao , Hongbin Wu , Dianxue Cao . Direct regeneration of spent LiFePO₄ cathode material via a simple solid-phase method. Chinese Chemical Letters, 2025, 36(6): 110041-. doi: 10.1016/j.cclet.2024.110041
6. [6]
  Feng Cui , Fangman Chen , Xiaochun Xie , Chenyang Guo , Kai Xiao , Ziping Wu , Yinglu Chen , Junna Lu , Feixia Ruan , Chuanxu Cheng , Chao Yang , Dan Shao . Scalable production of mesoporous titanium nanoparticles through sequential flash nanocomplexation. Chinese Chemical Letters, 2024, 35(4): 108681-. doi: 10.1016/j.cclet.2023.108681
7. [7]
  Keyang Li , Yanan Wang , Yatao Xu , Guohua Shi , Sixian Wei , Xue Zhang , Baomei Zhang , Qiang Jia , Huanhua Xu , Liangmin Yu , Jun Wu , Zhiyu He . Flash nanocomplexation (FNC): A new microvolume mixing method for nanomedicine formulation. Chinese Chemical Letters, 2024, 35(10): 109511-. doi: 10.1016/j.cclet.2024.109511
8. [8]
  Yiming Fang , Huimin Gao , Kaiting Cheng , Liang Bai , Zhengtong Li , Yadong Zhao , Xingtao Xu . An overview of photothermal materials for solar-driven interfacial evaporation. Chinese Chemical Letters, 2025, 36(3): 109925-. doi: 10.1016/j.cclet.2024.109925
9. [9]
  Xiao-Qian Wan , Ya-Ning Xu , Jian-Xin Yang , Dan Tian , Li-Long Dang , Feng Bai , Lu-Fang Ma . Structural optimization of organometallic cages for enhanced photothermal solar water evaporation. Chinese Journal of Structural Chemistry, 2025, 44(10): 100705-100705. doi: 10.1016/j.cjsc.2025.100705
10. [10]
  Chang Xu , Mengfan Luo , Jia Zhao , Jialong Yin , Can Feng , Heng Zhang , Peng Zhou , Zhaokun Xiong , Bo Lai . Ferrate(Ⅵ) combined with sulfur(Ⅳ) as an effective process for aromatic organoarsenic degradation: Essential role of Fe(Ⅲ) flocs. Chinese Chemical Letters, 2026, 37(4): 111538-. doi: 10.1016/j.cclet.2025.111538
11. [11]
  Chu Zeng , Han Yang , Ming Xu , Zhi-Yuan Gu . Optimizing COF crystallinity for high-resolution GC separation. Chinese Chemical Letters, 2026, 37(1): 110064-. doi: 10.1016/j.cclet.2024.110064
12. [12]
  Deqi Fan , Yicheng Tang , Yemei Liao , Yan Mi , Yi Lu , Xiaofei Yang . Two birds with one stone: Functionalized wood composites for efficient photocatalytic hydrogen production and solar water evaporation. Chinese Chemical Letters, 2024, 35(9): 109441-. doi: 10.1016/j.cclet.2023.109441
13. [13]
  Yuling Ma , Dongqing Liu , Tao Zhang , Chengjie Song , Dongmei Liu , Peizhi Wang , Wei Wang . Bimetallic composite carbon fiber with persulfate mediation for intercepting volatile organic compounds during solar interfacial evaporation. Chinese Chemical Letters, 2025, 36(3): 110000-. doi: 10.1016/j.cclet.2024.110000
14. [14]
  Shuangying Li , Qingxiang Zhou , Zhi Li , Menghua Liu , Yanhui Li . Sensitive measurement of silver ions in environmental water samples integrating magnetic ion-imprinted solid phase extraction and carbon dot fluorescent sensor. Chinese Chemical Letters, 2024, 35(5): 108693-. doi: 10.1016/j.cclet.2023.108693
15. [15]
  Xinyue Han , Yunhan Yang , Jiayin Lu , Yuxiang Lin , Dongxue Zhang , Ling Lin , Liang Qiao . Efficient serum lipids profiling by TiO₂-dopamin-assisted MALDI-TOF MS for breast cancer detection. Chinese Chemical Letters, 2025, 36(5): 110183-. doi: 10.1016/j.cclet.2024.110183
16. [16]
  Jinqi Yang , Xiaoxiang Hu , Yuanyuan Zhang , Lingyu Zhao , Chunlin Yue , Yuan Cao , Yangyang Zhang , Zhenwen Zhao . Direct observation of natural products bound to protein based on UHPLC-ESI-MS combined with molecular dynamics simulation. Chinese Chemical Letters, 2025, 36(5): 110128-. doi: 10.1016/j.cclet.2024.110128
17. [17]
  Mengyu Cao , Yiyan Yin , Jingyi Qin , Jin Ouyang , Na Na . Unconventional application of a fluorescent probe for MS-based detection of multiple sulfur species in ferroptosis. Chinese Chemical Letters, 2026, 37(1): 111260-. doi: 10.1016/j.cclet.2025.111260
18. [18]
  Guo-Ping Yin , Ya-Juan Li , Li Zhang , Ling-Gao Zeng , Xue-Mei Liu , Chang-Hua Hu . Citrinsorbicillin A, a novel homotrimeric sorbicillinoid isolated by LC-MS-guided with cytotoxic activity from the fungus Trichoderma citrinoviride HT-9. Chinese Chemical Letters, 2024, 35(8): 109035-. doi: 10.1016/j.cclet.2023.109035
19. [19]
  Pengyu Chen , Beibei Chen , Man He , Yuxi Zhou , Lei Lei , Jian Han , Bingsheng Zhou , Ligang Hu , Bin Hu . Nanoplastics and nano-ZnO facilitate Cd accumulation in zebrafish larvae via a distinct pathway: Revelation by LA-ICP-MS imaging. Chinese Chemical Letters, 2025, 36(2): 109908-. doi: 10.1016/j.cclet.2024.109908
20. [20]
  Dan Zhou , Liangjin Bao , Haoqi Long , Duo Zhou , Yuwei Xu , Bo Wang , Chuanqin Xia , Liang Xian , Chengbin Zheng . Capillary electrophoresis as sample introduction system for highly sensitive and interference-free determination of ⁹⁹Tc by ICP-MS. Chinese Chemical Letters, 2025, 36(4): 110093-. doi: 10.1016/j.cclet.2024.110093

Get Citation

PDF

XML

Metrics

PDF Downloads(1)
Abstract views(1345)
HTML views(29)

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142

Address：Zhongguancun North First Street 2,100190 Beijing, PR China Tel: +86-010-82449177-888

DownLoad: Full-Size Img PowerPoint

Return