Citation: Ze Yi YAN, Cheng Jin JIAO, Feng Min LI, Yong Min LIANG, Zhi Xiao LI. HPLC Determination of the Major Non-protein Amino Acids and Common Biogenic Amines in Lathyrus sativus Using a Novel Extraction Method[J]. Chinese Chemical Letters, ;2005, 16(5): 639-642. shu

HPLC Determination of the Major Non-protein Amino Acids and Common Biogenic Amines in Lathyrus sativus Using a Novel Extraction Method

1.
State Key Laboratory of Applied Organic Chemistry, Lanzhou University, Lanzhou 730000;
2.
School of Life Science, Lanzhou University, Lanzhou 730000

Received Date: 9 May 2004

Fund Project: This work was supported by NKBRSF Project (G2000018603) and the National Natural Science Foundation of China (No. 30270965).

An assay is presented for simultaneously determining 5 biogenic amines and the major non-protein amino acids:the toxin β-N-oxalyl-L-α,β-diaminopropanoic acid (β-ODAP), its isomer α-ODAP and homoarginine in Lathyrus sativus extracts using the HPLC system after derivatization with para-nitrobenzyloxycarbonyl chloride (PNZ-C1). However, it is more worthy of noting that this paper also describes a new extraction method using 0.2 mol/L HC1O₄. The new method has some advantages:shorter extraction-time, simultaneous extraction of free amino acids and polyamines, better inhibiting the isomerization of β-ODAP to α-ODAP, and so on.
- ODAP,
- homoginine,
- HPLC,
- biogenic amines,
- new extraction method
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