引用本文:
Duo Li, Hai Shen Yang, Qing Cui, Shen Jie Mao, Xiao Hua Xu. Synthesis of bacillamide 3 and its analogue[J]. Chinese Chemical Letters,
2009, 20(10): 1195-1197.
doi:
10.1016/j.cclet.2009.05.014
Citation: Duo Li, Hai Shen Yang, Qing Cui, Shen Jie Mao, Xiao Hua Xu. Synthesis of bacillamide 3 and its analogue[J]. Chinese Chemical Letters, 2009, 20(10): 1195-1197. doi: 10.1016/j.cclet.2009.05.014
Citation: Duo Li, Hai Shen Yang, Qing Cui, Shen Jie Mao, Xiao Hua Xu. Synthesis of bacillamide 3 and its analogue[J]. Chinese Chemical Letters, 2009, 20(10): 1195-1197. doi: 10.1016/j.cclet.2009.05.014
Synthesis of bacillamide 3 and its analogue
摘要:
The bacillamide 1 is a new algaecide from the marine bacterium Bacillus sp.SY-1.Its analogues bacillamide 3 and alkaloid 4 were firstly synthesized effectively from D-alanine.The key step was a coupling reaction via the mixed anhydride.All structures were confirmed by 1H NMR and 13C NMR.The final compounds were confirmed by 1HNMR,13C NMR and HRMS and the results are consistent with the reported natural products.
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关键词:
- Bacillamide
- / Thiazole rings
- / Tryptamide
- / Synthesis
English
Synthesis of bacillamide 3 and its analogue
Abstract:
The bacillamide 1 is a new algaecide from the marine bacterium Bacillus sp.SY-1.Its analogues bacillamide 3 and alkaloid 4 were firstly synthesized effectively from D-alanine.The key step was a coupling reaction via the mixed anhydride.All structures were confirmed by 1H NMR and 13C NMR.The final compounds were confirmed by 1HNMR,13C NMR and HRMS and the results are consistent with the reported natural products.
-
Key words:
- Bacillamide
- / Thiazole rings
- / Tryptamide
- / Synthesis
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