Citation: Li Li, Chun Ming Liu, Zhi Qiang Liu, Jing Wang. Isolation and purification of phenylethanoid glycosides from plant extract of Plantago asiatica by high performance centrifugal partition chromatography[J]. Chinese Chemical Letters, ;2008, 19(11): 1349-1352. doi: 10.1016/j.cclet.2008.09.002 shu

Isolation and purification of phenylethanoid glycosides from plant extract of Plantago asiatica by high performance centrifugal partition chromatography

a The Central Laboratory, Changchun Normal University, Changchun 130032, China;
b Laboratory of New Drug Research and Mass Spectrometry, Changchun Institute of Applied Chemistry, Changchun 130021, China

Received Date: 19 May 2008

Fund Project: This work was supported by funding from Jilin Province (No. 20060904-1 and 20071102).

Two phenylethanoid glycosides (PhGs) were isolated and purified from the aerial parts of Plantago asiatica for the first time by high performance centrifugal partition chromatography (HPCPC) using ethyl acetate-n-butanol-ethanol-water (0.5:0.5:0.1:1,v/v/v/v). A total of 45.6 mg of compound 1 and 293.8 mg of compound 2 were purified from 1341 mg of the n-butanol extract of P.asiatica.The structures of the two PhGs were tentatively identified as plantamajoside and acteoside or isoacteoside by electrospray ionization multi stage tandem mass spectrometry (ESI-MSⁿ) in the negative ion mode.
- Plantago asiatica L.,
- Pbenylethanoid glycosides,
- HPCPC,
- ESI-MSⁿ
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