引用本文:
Yu Xin LI, Zheng Ming LI, Wei Guang ZHAO, Wen Li DONG, Su Hua WANG. Synthesis of Novel 1-Arylsulfonyl-4-(1'-N-2', 3', 4', 6'-tetra-O-acetyl-β-D-glucopyranosyl)thiosemicarbazides[J]. Chinese Chemical Letters,
2006, 17(2): 153-155.
Citation: Yu Xin LI, Zheng Ming LI, Wei Guang ZHAO, Wen Li DONG, Su Hua WANG. Synthesis of Novel 1-Arylsulfonyl-4-(1'-N-2', 3', 4', 6'-tetra-O-acetyl-β-D-glucopyranosyl)thiosemicarbazides[J]. Chinese Chemical Letters, 2006, 17(2): 153-155.
Citation: Yu Xin LI, Zheng Ming LI, Wei Guang ZHAO, Wen Li DONG, Su Hua WANG. Synthesis of Novel 1-Arylsulfonyl-4-(1'-N-2', 3', 4', 6'-tetra-O-acetyl-β-D-glucopyranosyl)thiosemicarbazides[J]. Chinese Chemical Letters, 2006, 17(2): 153-155.
Synthesis of Novel 1-Arylsulfonyl-4-(1'-N-2', 3', 4', 6'-tetra-O-acetyl-β-D-glucopyranosyl)thiosemicarbazides
摘要:
The synthesis of novel 1-arylsulfonyl -4-(1'-N-2', 3', 4', 6'-tetra-O-acetyl-β-D-glucopyranosyl) thiosemicarbazides via condensation of 2, 3, 4, 6-tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate with substituted phenylsulfonyl hydrazines was described. Their structures and physical properties were confirmed by 1H NMR, 13C NMR spectra, elemental analysis and MS.
English
Synthesis of Novel 1-Arylsulfonyl-4-(1'-N-2', 3', 4', 6'-tetra-O-acetyl-β-D-glucopyranosyl)thiosemicarbazides
Abstract:
The synthesis of novel 1-arylsulfonyl -4-(1'-N-2', 3', 4', 6'-tetra-O-acetyl-β-D-glucopyranosyl) thiosemicarbazides via condensation of 2, 3, 4, 6-tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate with substituted phenylsulfonyl hydrazines was described. Their structures and physical properties were confirmed by 1H NMR, 13C NMR spectra, elemental analysis and MS.
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Key words:
- Phenylfulfonyl hydrazine
- / thiosemicarbazide
- / condensation
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