Synthesis of 1,1'-binaphthyl-2,2'-diamine from 2-naphthol under atmospheric pressure

Qiang Feng Chao Zhang Qiang Tang Mei Ming Luo

引用本文: Qiang Feng,  Chao Zhang,  Qiang Tang,  Mei Ming Luo. Synthesis of 1,1'-binaphthyl-2,2'-diamine from 2-naphthol under atmospheric pressure[J]. Chinese Chemical Letters, 2009, 20(10): 1150-1152. doi: 10.1016/j.cclet.2009.05.033 shu
Citation:  Qiang Feng,  Chao Zhang,  Qiang Tang,  Mei Ming Luo. Synthesis of 1,1'-binaphthyl-2,2'-diamine from 2-naphthol under atmospheric pressure[J]. Chinese Chemical Letters, 2009, 20(10): 1150-1152. doi: 10.1016/j.cclet.2009.05.033 shu

Synthesis of 1,1'-binaphthyl-2,2'-diamine from 2-naphthol under atmospheric pressure

  • 基金项目:

    We are grateful to National Natural Science Foundation of China (No.20372049) and Application Basic Research Funding of Sichuan.We also thank Analytical & Testing Center of Sichuan University for support in NMR and MS analyses.

摘要: A practical protocol to obtain 1,1'-binaphthyl-2,2'-diamine was developed from 2-naphthol and 2-naphthylhydrazine under mild conditions:solvent-free, 125-130℃, atmospheric pressure.The convenient procedure makes the process amenable for large-scale synthesis of the versatile compound.

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  • 收稿日期:  2009-02-12
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