Solvent-free and catalyst-free method for the synthesis of 2,4,5-triarylimidazoles under microwave irradiation

Jian Feng Zhou Gui Xia Gong Hui Qin Zhu Feng Xia Zhu

引用本文: Jian Feng Zhou,  Gui Xia Gong,  Hui Qin Zhu,  Feng Xia Zhu. Solvent-free and catalyst-free method for the synthesis of 2,4,5-triarylimidazoles under microwave irradiation[J]. Chinese Chemical Letters, 2009, 20(10): 1198-1200. doi: 10.1016/j.cclet.2009.05.027 shu
Citation:  Jian Feng Zhou,  Gui Xia Gong,  Hui Qin Zhu,  Feng Xia Zhu. Solvent-free and catalyst-free method for the synthesis of 2,4,5-triarylimidazoles under microwave irradiation[J]. Chinese Chemical Letters, 2009, 20(10): 1198-1200. doi: 10.1016/j.cclet.2009.05.027 shu

Solvent-free and catalyst-free method for the synthesis of 2,4,5-triarylimidazoles under microwave irradiation

  • 基金项目:

    We thank the Jiangsu Key Laboratory for Chemistry of Low-Dimensional Materials for financial support (No.JSKC07041)

摘要: A facile procedure for the synthesis of 2,4,5-triarylimidazoles is being reported starting from benzil, aromatic aldehyde and ammonium acetate.The reactions were carried out with catalyst-free, solvent-free and under microwave irradiation conditions in high yield (80-99%) with short time (3-5 min) and environmental benign, as well as convenient operation.The structures of the compounds have been confirmed on the basis of their IR,1H NMR, and/or 13C NMR, MS, and elemental analyzer.

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  • 收稿日期:  2009-03-09
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